A microwave-heated infrared reaction cell for the in-situ study of heterogeneous catalysts

  • Ian Silverwood Edinburgh University-Reino Unido
  • Gordon McDougall Edinburgh University-Reino Unido
  • Gavin Whittaker Edinburgh University-Reino Unido

Abstract

A transmission infrared microreactor cell which holds a catalyst pressed disc in a controlled atmosphere and allows microwave and conventional heating up to 423K is demonstrated using the oxidation of carbon monoxide over the standard catalyst, EUROPT- 1. Optical characteristics are determined by the choice of CaF2, as the window material, allowing transmission from 77000- 1000cm-1. An oscillating microwave power heating regime with a peak height of 200W is used and time-resolved infrared spectra and mass spectrometry show oscillations in the reaction which correspond to the microwave heating.

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How to Cite
Silverwood, I., McDougall, G., & Whittaker, G. (1). A microwave-heated infrared reaction cell for the in-situ study of heterogeneous catalysts. Ciencia, 14. Retrieved from https://mail.produccioncientificaluz.org/index.php/ciencia/article/view/9579
Issue
Vol. 14: Edición Especial
Section
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